R-Axis Spider Area Detector System (single crystals and powders)

XRD02

CONTACT PERSON:

Dr. Vasilis Psycharis

EMAIL:

v.psycharis@inn.demokritos.gr

CONTACT PERSON:

Dr. C. P. Raptopoulou

EMAIL:

c.raptopoulou@inn.demokritos.gr

XRD /X-Ray Diffraction

Tool
R-axis Spider Single Crystal diffractometer

Applications
Single Crystal data collection, powder samples (capillarymounting)

Technical SpecificationsSource: Cu, Mo, Fe, Co radiation
Geometry: Tree circle goniometer
Optics: collimators (conventional and capillary optics), primary pyrolytic graphite monochromator

Detectors: scintillation detector Image plate (2D) large area
-Goniometer heads for sample mounting-X-Sream 2000,Low temperature unit, with Nitrogen generator, He compressor, stainless steel hose and nozzle for delivery of nitrogen on the sample.
Temperature range operation: 100K-RT.
-Measurement of single crystals with 1mm size and smaller and powder samples in capillaries

Analysis Software: Crystal Clear, WINGX(GUI), OLEX-2(GUI), SIR, SHELXS-SHELXL, CrystalExplorer (intermolecular Interactions Studies)

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